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This electrophile will be reacted with 3,5-dimethoxyphenol in an Interrupted Feist-Bénary-like reaction to synthesize the backbone of nigropsine. Nigrospine is a natural product that has potent antifungal properties making it a promising target. Additionally, nigrospine has never seen synthetic work before, and this thesis outlines the importance of synthesizing it as well as progress towards it synthesis. The desired electrophile is a tricarbonyl lactam derived from alanine. This thesis explores several approaches to synthesize the tricarbonyl lactam from the dicarbonyl lactam. While the target electrophile was not successfully synthesized, great progress was made towards it including the synthesis of a lactam with two carbonyls and a hydroxyl group. This thesis also explores a tricarbonyl lactone electrophile derived from ascorbic acid that could be converted later to a lactam. Additionally, this thesis outlines future studies towards synthesizing the desired lactam and nigrospine.</p>"},{"label":"Digital Identifier","value":"m2023-g677"},{"label":"Thesis Advisor(s)","value":["Calter, Michael A."]},{"label":"Digital Object Identifier (DOI)","value":"https://doi.org/10.14418/wes01.2.398"},{"label":"Discipline","value":["Chemistry"]},{"label":"Date","value":"December 15, 2022"},{"label":"EDTF Date","value":"D:00 M:00 Y:2022"},{"label":"Extent","value":"v, 62 pages : illustrations, charts ; 28 cm"},{"label":"File Format","value":["application/pdf"]},{"label":"Genre","value":["masters theses"]},{"label":"Digital Origin","value":["born digital"]},{"label":"Type","value":["Text"]}],"description":"Progress towards the synthesis of 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