{"@context":"http://iiif.io/api/presentation/2/context.json","@type":"sc:Manifest","@id":"https://iiif.quartexcollections.com/wesleyan/iiif/9a10ce86-6460-4167-8ad8-cc16d45dd1ab/manifest","label":"m2021-w246","metadata":[{"label":"Title","value":"The optimization of several one-pot syntheses of shaped palladium-silver nanoparticles and preliminary catalytic studies on their selective hydrogenation of 1-hexyne"},{"label":"Subject","value":["Hydrogenation","Metal nanoparticles"]},{"label":"Rights","value":["In Copyright"]},{"label":"Repository","value":["University Archives"]},{"label":"Language","value":["English"]},{"label":"Item Information","value":"<a href=\"https://onesearch.wesleyan.edu/permalink/01CTW_WU/12cbh08/alma9932796975603768\" target=\"_blank\">M2021 W246</a>"},{"label":"Held By","value":"Wesleyan University Library, Wesleyan University, Middletown, CT, USA"},{"label":"Group","value":["Theses & Dissertations"]},{"label":"Name(s)","value":["Wang, Jing Jang (creator)"]},{"label":"Administrative Note","value":"Node ID: 17150<br>Author Contact: cwang@wesleyan.edu<br>Local Identifier: Wang_JingJing_Item_11_2Copies<br>PID: ir:3046"},{"label":"Author-supplied Keywords","value":["1-hexyne","Selective hydrogenation","Palladium-silver","Synthesis","Catalysis","Bimetallic","Silver","Palladium","Nanoparticles"]},{"label":"Degree","value":["Master of Arts"]},{"label":"Description","value":"<p>Due to the increasing demand for synthetic products, the chemical industry is projected to be responsible for a third of the growth in energy demand between 2017 to 2040 in a study by Exxon Mobil. The challenge of mitigating this energy demand can be addressed using catalysis and catalyst development since catalysts are used in most industrial chemical transformations. Nanoparticles, especially bimetallic and multimetallic nanoparticles, are promising materials due to their small size and adaptable shape and surface structure, leading to tailorable catalytic properties. Exploring the pathways to achieve homogeneous, shaped metal nanoparticles with desirable properties is advantageous for lowering energy demand in catalytic transformations. This thesis will focus on the one-step synthesis and optimization of palladium-silver nanoparticles and testing the catalytic properties of each optimized particle shape in the selective hydrogenation of 1-hexyne. Chapter One introduces the motivation and the broader goals and implications of this research. It highlights key ideas and concepts that are crucial for understanding the methods and variables that influence nanoparticle growth. Chapter Two briefly reiterates the challenges of synthesizing palladium-silver nanoparticles via two-step methods and investigates a versatile one-step approach using underpotential deposition conditions. Chapter Two also briefly introduces preliminary catalytic data for palladium and palladium-silver particles. The selective hydrogenation of 1-hexyne, specifically, is studied to understand and model the behavior of palladium-silver catalysts for future applications in more complex catalytic reactions. Overall, this thesis proposes improved conditions for various one-step palladium particle syntheses and analyzes the behavior of palladium and palladium-silver catalysts with the goal of better understanding the mechanisms that control nanoparticle growth and how nanoparticle properties influence their catalytic behavior.</p>"},{"label":"Digital Identifier","value":"m2021-w246"},{"label":"Thesis Advisor(s)","value":["Personick, Michelle L."]},{"label":"Digital Object Identifier (DOI)","value":"https://doi.org/10.14418/wes01.2.315"},{"label":"Discipline","value":["Chemistry"]},{"label":"Date","value":"May 11, 2021"},{"label":"EDTF Date","value":"D:00 M:00 Y:2021"},{"label":"Extent","value":"x, 68 pages : illustrations ; 28 cm"},{"label":"File Format","value":["application/pdf"]},{"label":"Genre","value":["masters theses"]},{"label":"Digital Origin","value":["born digital"]},{"label":"Type","value":["Text"]}],"description":"The optimization of several one-pot syntheses of shaped 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