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However, their commercial viability is hindered by halide segregation, a reversible illumination-induced phenomenon that leads to spatial inhomogeneity in band structure and degrades device performance. This thesis aims to explore the process of halide segregation in mixed halide perovskites through the lens of confocal microscopy, a unique technique that offers both spectral and spatial resolution. This involved performing three analyses. First, we used wavelength-resolved confocal scans to compare the spectral evolution of MA-based and CsFA-based perovskites under illumination. We found that MA-based samples exhibited significantly greater instability, which is consistent with existing literature. Next, we developed a spatially-resolved grain classification framework to identify local variations in emission behavior across individual perovskite grains. Applying this method to an MA-based sample with high bromide content, we identified four distinct grain types based on their emission dynamics and found that iodide-rich domains emerged in spatially coherent clusters, often originating from defect-rich regions. Adjacency analysis confirmed the spatial clustering of these grain types and suggested that halide segregation propagates across grain boundaries or interfaces. Finally, we investigated the effects of repeated illumination by scanning the same region of a triple-halide sample across multiple excitation cycles. We observed that segregation rates increased with each cycle, while iodide-rich regions gradually diminished, indicating cumulative and partially irreversible changes in both spectral and spatial emission behavior. We conclude by discussing our findings in detail and proposing potential future experiments, as well as potential improvements to our current analytical approaches.</p>"},{"label":"Group","value":["Theses & Dissertations"]},{"label":"Digital Origin","value":["born digital"]},{"label":"Discipline","value":["Physics"]},{"label":"Date","value":"April 15, 2025"},{"label":"EDTF Date","value":"D:00 M:00 Y:2025"},{"label":"File Format","value":["application/pdf"]},{"label":"Digital Object Identifier (DOI)","value":"https://doi.org/10.14418/wes01.1.3190"},{"label":"Type","value":["Text"]}],"description":"Analyzing halide segregation in mixed halide perovskites using confocal microscopy and grain type 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