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Consolidating the terminal alkyne and halide reactive ends into a single AB type monomer could drastically increase the degree of polymerization for the CO2 polymerization system. Additionally, determining if polymerization is possible without a conjugated terminal alkyne could deepen the reservoir of possible starting materials for these polymerizations. Here, we aimed to understand the relationship between structure and polymerization by functionalizing bio-based molecules into AB type monomers and polymerizing them using optimized conditions from literature precedent and our own studies. From small molecule studies primarily using vanillin and 4-hydroxybenzaldehyde, we determined that a conjugated terminal alkyne is not strictly necessary for successful polymerizations, and that the alkyl halide should be placed on an extended aliphatic chain. These small molecule findings were corroborated during the functionalization and polymerization of our AB type monomers. These findings have expanded the library of possible bio- based polymer starting materials and helped in understanding the fundamental necessities for the development of functional polyesters from CO2.</p>"},{"label":"Digital Identifier","value":"b2026-Larson"},{"label":"Digital Object Identifier (DOI)","value":"https://doi.org/10.14418/9p8agf9j"},{"label":"Digital Origin","value":["born digital"]},{"label":"Discipline","value":["Chemistry"]},{"label":"Date","value":"April 15, 2026"},{"label":"EDTF Date","value":"D:00 M:00 Y:2026"},{"label":"File Format","value":["application/pdf"]},{"label":"Genre","value":["theses"]},{"label":"Group","value":["Theses & Dissertations"]},{"label":"Held By","value":"Wesleyan University Library, Wesleyan University, Middletown, CT, USA"},{"label":"Language","value":["English"]},{"label":"Repository","value":["University Archives"]},{"label":"Rights","value":["In Copyright"]},{"label":"Thesis Advisor(s)","value":["Elling, 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